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- "Green" HPLC with 100% Water Eluent for Analysing Melamine in Milk
Naoto Furusawa, Eriko Tsumatani
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A reversed-phase (RP) high performance liquid chromatography (HPLC) method for analysing melamine residue in cow's milk using 100% water
in the sample preparation stage and as the eluent is described. HPLC was performed on an ODS column with an isocratic 100% water mobile
phase and a photo-diode array (PDA) detector. The proposed method was validated by the analyses of spiked milk samples resulting in
recoveries greater than 96.8% with a relative standard deviation (RSD) of less than 2.0%. The total analysis time was less
than 15 min/sample and the quantitation limit was 0.05 µg/g.
LCGC Europe, Jun 1, 2012
Column: ODS 4
- Determination of airborne particle-associated benz[a]anthracene-7,12-quinone using high-performance liquid chromatography with in-line reduction and fluorescence detection
Takayuki Kameda, Tomoko Goto, Akira Toriba, Ning Tang, Kazuichi Hayakawa
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Institute of Medical, Pharmaceutical and Health Sciences, Kanazawa University Kakuma-machi, Kanazawa, Ishikawa 920-1192, Japan.
Journal of Chromatography A, 1216, 2009 6758-6761
Column: a separation column Inertsil ODS-EP, 2.1mm ID×250mm, a trapping column Inertsil ODS-3, 4.0mm ID×30mm
- Development of a high-performance liquid chromatography – fluorescence detection method for analyzing nonylphenol/dinonylphenol-polyethoxylate-based phosphate esters
Ake Stenholm, Sara Holmstrom, Sandra Hjarthag, Ola Lind
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Quality Control Support, GE Healthcare, Björkgatan 30, S-751 84 Uppsala, Sweden
Journal of Chromatography A, In Press 2009 Available online 27 August
Column:Inertsil PH
- Liquid chromatographic analysis of Hg(II) binding by thiol-rich peptides using both UV-vis and electrochemical detection.
Àngela Dago, Olga González-García, Cristina Ariño, José Manuel Díaz-Cruz, Miquel Esteban
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Departament de Química Analítica. Facultat de Química. Universitat de Barcelona (UB) Martí i Franquès, 1-11, E – 08028 – Barcelona (Spain)10 55455
Journal of Chromatography A, 1216 2009, 6752-6757
Column:C18 Inertsil ODS-2, particle size 5µm, 250mm×4.6mm
- Application of Snyder-Dolan Classification Scheme to the Selection of “Orthogonal” Columns for Fast Screening for Illicit Drugs and Impurity Profiling of Pharmaceuticals.
Wenzhe Fan, Yu Zhang, Peter W. Carr, Sarah C. Rutan, Melanie Dumarey, Adam P. Schellinger, Wayne Pritts
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University of Minnesota, Department of Chemistry, 207 Pleasant Street SE, Minneapolis, MN, 105 55455, USA
Journal of Chromatography A, 1216 2009, 6587-6599
Column:ODS-2, particle size 5µm, 250mm×4.6mm
- Method performance and multi-laboratory assessment of a normal phase high pressure liquid chromatography–fluorescence detection method for the quantitation of flavanols and procyanidins in cocoa and chocolate containing samples
Rebecca J. Robbinsa, Jadwiga Leonczaka, J. Christopher Johnsona, Julia Li a, Catherine Kwik-Uribea, Ronald L. Priorb, Liwei Guc
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Analytical and Applied Sciences Group, Mars, Incorporated, 800 High Street Hackettstown, NJ 07840, United States
Journal of Chromatography A, 1216 2009, 4831–4840
Column:Inertsil
- Controllable shape selectivity based on highly ordered carbonyl and methyl groups in simple [1]-structural polypeptide on silica
Atsuomi Shundo, Abul K. Mallik, Toshihiko Sakurai, Makoto Takafuji, Shoji Nagaoka, Hirotaka Iharaa,
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Department of Applied Chemistry and Biochemistry, Kumamoto University, 2-39-1 Kurokami, Kumamoto 860-8555, Japan
Journal of Chromatography A, 1216 -2009, 6170–6176
Column:Inertsil ODS-3, 250mm×4.6mm I.D
- Improvement of separation efficiencies of anion-exchange chromatography using monolithic silica capillary columns modified with polyacrylates and polymethacrylates containing tertiary amino or quaternary ammonium groups
Yuta Watanabe, Tohru Ikegami, Kanta Horie, Takeshi Hara, Jafariah Jaafar, Nobuo Tanaka
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Department of Biomolecular Engineering, Kyoto Institute of Technology, Matsugasaki, Sakyo-ku, Kyoto 606-8585, Japan
Journal of Chromatography A, In Press, 2009 Available online 14 July
Column:Inertsil AX (5 µm, 100 Å, 250 mm × 3.0 mm I.D.)
- A Visual Approach to Stationary Phase Selectivity Classification Based on the Snyder-Dolan Hydrophobic-Subtraction Model
Yu Zhang and Peter W. Carr
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Department of Chemistry, University of Minnesota,Smith and Kolthoff Hall, 207 Pleasant Street SE, Minneapolis, MN 55455
Journal of Chromatography A, 1216, 2009, 6685-6694
Column:Inertsil ODS, Ph, CN
- Aqueous chromatographic system for the quantification of propofol in biological fluids using a temperature-responsive polymer modified stationary phase
Tadashi Nishio, Rie Suzuki, Yuko Tsukada, Hideko Kanazawa, Teruo Okano, Takako Miyabe-Nishiwaki
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Faculty of Pharmacy, Keio University, 1-5-30, Shibakoen, Minato-ku, Tokyo 105-8512, Japan
Journal of Chromatography A, In Press, 2009 Available online 21 April
Column:Inertsil ODS-3 5µm, 150mm×4.6mm I.D.
- Poly(2-N-carbazolylethyl acrylate)-modified silica as a new polymeric stationary phase for reversed-phase high-performance liquid chromatography
Usha Ghimire Gautam, Tsuyoshi Sawada, Mani Prasad Gautam, Makoto Takafuji, Hirotaka Ihara
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Department of Applied Chemistry and Biochemistry, Kumamoto University, 2-39-1 Kurokami, Kumamoto 860-8555, Japan
Journal of Chromatography A, In Press, 2009 Available online 18 April
Column:Monomeric ODS Inertsil ODS-3, 250mm×4.6mm I.D
- Selecting an “orthogonal” column during high-performance liquid chromatographic method development for samples that may contain non-ionized solutes
J.W. Dolan, L.R. Snyder
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LC Resources Inc., 15664 SE Woodland Hts, Amity, OR 97101, USA
Journal of Chromatography A, 1216 -2009 3467–3472
Column:Inertsil ODS, CN
- Thermodynamic investigations on shape selective separation behaviors of poly(4-vinylpyridine)-grafted silica for polycyclic aromatic hydrocarbons in both normal-phase and reversed-phase high-performance liquid chromatography
Usha Ghimire Gautam, Mani Prasad Gautam, Tsuyoshi Sawada, Makoto Takafuji, Hirotaka Ihara
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Department of Applied Chemistry and Biochemistry, Kumamoto University, 2-39-1 Kurokami, Kumamoto 860-8555, Japan
Journal of Chromatography A, 1216 -2009, 3571–3577
Column:Monomeric ODS Inertsil ODS-3, 250mm×4.6mm I.D
- Improvement of sensitivity and selectivity of high-performance liquid chromatography for anti-retroviral drugs (non-reverse transcriptase inhibitors) by diamond-electrode electrochemical and fluorescence detection
Katsuhiro Suzukia, Masatoki Katayama, Kiyoshi Takamatsuc, Satoru Kanekoc, Keisuke Miyaji, Hiromichi Ishikawa, Yoshifumi Matsuda
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Department of Drug Metabolism Research Laboratories, Drug Discovery Research, Astellas Pharma Inc., 1-1-8 Azusawa, Itabashi-ku, Tokyo 174-8511, Japan b Department of Functional Bioanalysis, Meiji Pharmaceutical University, 2-522-1, Noshio, Kiyose, Tokyo 204-8588, Japan
Journal of Chromatography A, 1216 -2009, 3117–3121
Column:Inertsil ODS-2, ED 605 pulse ED system
- Evaluation of two approaches to characterise liquid chromatographic columns using pharmaceutical separations
Sanja Dragovic, Erik Haghedooren, Tamás Németha, I. Murat Palabiyika, Jos Hoogmartens, Erwin Adams
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Katholieke Universiteit Leuven, Laboratorium voor Farmaceutische Analyse, O&N 2, PB 923, Herestraat 49, B-3000 Leuven, Belgium
Journal of Chromatography A, 1216 -2009, 3210–3216
Column:Inertsil ODS2 250 4.6 5 150, Inertsil ODS3 250 4.6 5 100, Inertsil ODS80Å
- Different sample stacking strategies for the determination of ertapenem and its impurities by micellar electrokinetic chromatography in pharmaceutical formulation
Katarzyna Michalska, Genowefa Pajchel, Stefan Tyskia
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Department of Antibiotics and Microbiology, National Medicines Institute, Che?mska 30/34, 00-725 Warsaw, Poland
Journal of Chromatography A, 1216 -2009, 2934–2942
Column:Inertsil Phenyl 5µ (250mm×4.6mm i.d.)
- Chemical analysis and quality control of Ginkgo biloba leaves, extracts, and phytopharmaceuticals
Teris A. van Beek, Paola Montoro
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Laboratory of Organic Chemistry, Natural Products Chemistry Group, Wageningen University, Dreijenplein 8, 6703 HB Wageningen, The Netherlands
Journal of Chromatography A, 1216 -2009, 2002–2032
Column:Inertsil ODS-3 150mm×4.6mm, 5µ
- Retention models for ionizable compounds in reversed-phase liquidchromatography Effect of variation of mobile phase composition and temperature
Martí Rosés, Xavier Subirats, Elisabeth Bosch
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Departament de Química Analítica, Universitat de Barcelona, Martí i Franquès 1-11, E-08028 Barcelona, Spain
Journal of Chromatography A, 1216 -2009 1756–1775
Column:Inertsil ODS 3V
- High through-put aflatoxin determination in plant material by automated solid-phase extraction on-line coupled to laser-induced fluorescence screening and determination by liquid chromatography–triple quadrupole mass spectrometry
M. Alcaide-Molina, J. Ruiz-Jiménez, J.M. Mata-Granados, M.D. Luque de Castro
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Department of Analytical Chemistry, Annex Marie Curie Building, Campus of Rabanales, University of Córdoba, E-14071, Córdoba, Spain b SANYRES (GRUPO PRASA), E-14012, Córdoba, Spain
Journal of Chromatography A, 1216 -2009 1115–1125
Column:Inertsil ODS–2 (4.6mm×250mm; 5µm )
- Analytical methods for the determination of bisphenol A in food
Ana Ballesteros-Gómez, Soledad Rubio, Dolores Pérez-Bendito
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Department of Analytical Chemistry, Facultad de Ciencias, Edificio Anexo Marie Curie, Campus de Rabanales, 14171 Córdoba, Spain
Journal of Chromatography A, 1216 -2009 449–469
Column:Inertsil ODS-2, 150mm×4.6mm I.D., 5µm
- Liquid chromatography–tandem mass spectrometric analysis and regulatory issues of polar pesticides in natural and treated waters
Marina Kuster, Maria López de Alda, Damià Barceló
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Department of Environmental Chemistry, IDAEA-CSIC, Jordi Girona 18-26, 08034 Barcelona, Spain b Catalan Institute for Water Research (ICRA), Parc Científic i Tecnològic de la Universitat de Girona, Edifici Jaume Casademont, E-17003 Girona, Spain
Journal of Chromatography A, 1216 -2009 520–529
Column:Inertsil ODS-2 (250×4.6mm, 5µm)
- Improved liquid chromatography tandem mass spectrometry method for the determination of phenolic compounds in virgin olive oil
Manuel Suárez, Alba Macià, Maria-Paz Romero, Maria-José Motilva
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Food Technology Department, CeRTA-TPV, Escuela Técnica Superior de Ingeniería Agraria, Universidad de Lleida, Av/Alcalde Rovira Roure 191, 25198 Lleida, Spain
Journal of Chromatography A, 1214 -2008 90–99
Column:Inertsil ODS-3 column (5µm, 15cm×4.6mm)
- Development of an automated on-line pre-column derivatization procedure for sensitive determination of histamine in food with high-performance liquid chromatography–fluorescence detection
Jin-feng Peng, Ke-teng Fang, Dong-hua Xie, Bin Ding, Ju-Yi Yin, Xiao-mei Cui, Ying Zhang, Jing-fu Liu
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Ningbo Entry-Exit Inspection and Quarantine Bureau, Ningbo 315012, China. State Key Laboratory of Environmental Chemistry and Ecotoxicology, Research Center for Eco-Environmental Sciences, Chinese Academy of Sciences, P.O. Box 2871, Beijing 100085, China
Journal of Chromatography A, 1209 -2008 70–75
Column:Cloversil C18 column, Inertsil ODS-3 column and Waters Xbridge C18 column
- Anion-exchange behavior of several alkylsilica reversed-phase columns
D.H. Marchand, L.R. Snyder
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Department of Chemistry, University of Wisconsin-River Falls, River Falls, WI 54022, USA
Journal of Chromatography A, 1209 -2008 104–110
Column:Hypersil-100 C18 Alltima C18 HxSil C18 Ultra C18 Alltima HP C18 Nucleodur 100-C18 Prodigy ODS(3) 100A Prodigy ODS(2) J’Sphere ODS-L80 80A Symmetry C18 1.87 Luna C18 100A 2.81 Sunfire C18 2.84 Inertsil ODS-3 Xterra MS C18 Amino-end-capped column Spherisorb ODSB
- Novel two-dimensional reversed-phase liquid chromatography/hydrophilic interaction chromatography, an excellent orthogonal system for practical analysis
Yanming Liu, Zhimou Guo, Yu Jin, Xingya Xue, Qing Xu, Feifang Zhang, Xinmiao Liang
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Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian, Liaoning 116023, China
Journal of Chromatography A, 1208
Column:C18 column (Inertsil ODS-3, 5µ)
- Click oligo(ethylene glycol): An excellent orthogonal stationary phase to C18 for two-dimensional reversed-phase/reversed-phase liquid chromatography
Yanming Liu, Zhimou Guo, Yu Jin, Xingya Xue, Qing Xu, Feifang Zhang, Xinmiao Liang
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Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 457 Zhongshan Road, Dalian, Liaoning 116023, China
Journal of Chromatography A, 1206 -2008 153–159
Column:CN column (Inertsil CN-3, 5µm, 250mm×4.6mm i.d.), XTerra MS C18 column (5µm, 150mm×2.1mmi.d.) and Click OEG column (5µm, 150mm×4.6mm i.d., laboratory-made).
- Optimized conditions for high-performance liquid chromatography analysis of oligosaccharides using 7-amino-4-methylcoumarin as a reductive amination reagent
Masahiro Yodoshi, Akiko Tani, Yumiko Ohta, Shigeo Suzuki
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School of Pharmacy, Kinki University, 3-4-1, Kowakae, Higashi-osaka 577-8502, Japan
Journal of Chromatography A, 1203 -2008 137–145
Column:15cm×6mm I.D., Inertsil ODS-3
- Preparation, telomerization, immobilization and application of N-alkyl l-phenylalanine-derived polymerizable organogelator for reversed-phase high-performance liquid chromatography
M. Mizanur Rahman, Makoto Takafuji, Hirotaka Ihara
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Department of Applied Chemistry and Biochemistry, Faculty of Engineering, Kumamoto University, 2-39-1 Kurokami, Kumamoto 860-8555, Japan
Journal of Chromatography A, 1203 -2008 59–66
Column:ODS (monomeric) (Inertsil ODS, i.d. 250mm×4.6mm)
- Study of vacuum microwave-assisted extraction of polyphenolic compounds and pigment from Chinese herbs
Jun-XiaWang, Xiao-Hua Xiao, Gong-Ke Li
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School of Chemistry and Chemical Engineering, Sun Yat-sen University, Xingang West Road 135, Guangzhou 510275, China
Journal of Chromatography A, 1192 -2008 54–61
Column:SB-C18 , wide pore SB-C18, Extend-C18 Agilent Technologies. Alltima C18 ACEC18, Discovery HC-C18 and Inertsil ODS-3 (90 Å pore size)
- Characterization and applications of reversed-phase column selectivity based on the hydrophobic-subtraction model
D.H. Marchand, L.R. Snyder, J.W. Dolan
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niversity of Wisconsin-River Falls, River Falls, WI 54022-5001, USA and LC Resources, 15664 SE Woodland Hts., Amity, OR 97101, USA
Journal of Chromatography A, 1191 -2008 2–20
Column:250mm×4.6mm Inertsil ODS-2 column (type-B); Inertsil CN-3
- Contribution of sulfonyl–aromatic and sulfonic acid–aromatic interactions in novel sulfonyl/sulfonic acid-embedded reversed phase materials
Jeannie Horak, Wolfgang Lindner
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Institute of Analytical Chemistry, University of Vienna, Waehringer strasse 38, 1090 Vienna, Austria
Journal of Chromatography A, 1191 -2008 141–156
Column:Inertsil ODS-3 150mm×3 mm, With the increase of µ-interaction properties in the order Inertsil C18 < C3-S-C14 e.c. < C3-S-C18/SH < C3-SO2-C14 e.c. < C3-SO2-C18/SO3H
- Aqueous chromatographic system for separation of biomolecules using thermoresponsive polymer modified stationary phase
Hideko Kanazawa, Mayumi Nishikawa, Aya Mizutani, Chikako Sakamoto, Yuko, Morita-Murase, Yoshiko Nagata, Akihiko Kikuchi, Teruo Okanoc
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Department of Physical Pharmaceutical Chemistry, Kyoritsu University of Pharmacy, 1-5-30 Shibakoen, Minato-ku, Tokyo 105-8512, Japan
Journal of Chromatography A, 1191 -2008 157–161
Column:C18 column (Inertsil ODS-3, 150mm×4.6mm I.D., GL Science)
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